6'-Benzyloxy4',5'-dimethoxy-2,6-dimethyl-2'-methylbenzophenone → 6'-Butoxy-2,6-dichloro-4',5'-dimethoxy-2'-methylbenzophenone

HRID 1934309Notes

Reaction equation

HRID 1934309 reaction equation
[Cl:1][C:2]1[CH:29]=[CH:28][CH:27]=[C:26]([Cl:30])[C:3]=1[C:4]([C:6]1[C:11]([O:12][CH2:13][C:14]2C=CC=[CH:16][C:15]=2F)=[C:10]([O:21][CH3:22])[C:9]([O:23][CH3:24])=[CH:8][C:7]=1[CH3:25])=[O:5].C(OC1C(C(=O)C2C(C)=CC=CC=2C)=C(C)C=C(OC)C=1OC)C1C=CC=CC=1>>[CH2:13]([O:12][C:11]1[C:6]([C:4](=[O:5])[C:3]2[C:2]([Cl:1])=[CH:29][CH:28]=[CH:27][C:26]=2[Cl:30])=[C:7]([CH3:25])[CH:8]=[C:9]([O:23][CH3:24])[C:10]=1[O:21][CH3:22])[CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 227199526'-Benzyloxy4',5'-dimethoxy-2,6-dimethyl-2'-methylbenzophenoneHCID 227199542,6-Dichloro4',5'-dimethoxy-6'-(2-fluorobenzyloxy)-2'-methylbenzophenone

Product 1

HCID 227199566'-Butoxy-2,6-dichloro-4',5'-dimethoxy-2'-methylbenzophenone

Procedure

2,6-dichloro-4′,5′-dimethoxy-6′-(2-fluorobenzyloxy)-2′-methylbenzophenone (coded BB-2); 6′-benzyloxy-4′,5′-dimethoxy-2,6-dimethyl-2′-methylbenzophenone (coded BB-3); and 3-bromo-2′,6-dimethyl-2,40 ,5′,6′-tetramethoxybenzophenone (coded BB-4).

Sources & evidence

ORD record
ord-39e2e0c72906429493a821599e86a26a
Source dataset
uspto-grants-2002_05
Patent number
US06383984B1

Reaction notes

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