HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18738443, compound → HCID 18738434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18738443 | HCID 18738443 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18738434 | HCID 18738434 | — |
Reaction Steps
A 100 mL Fisher/Porter vessel was charged with 1 g of benzyl 3-(1-piperidinyl)sulfonyl-2(R)-methylpropionate 30 mL MeOH and a catalytic amount of 10% Pd—C. The reaction was hydrogenated at 50 psi for 3 hours. After filtration through Celite and concentration in vacuo of 3-(1-piperidinyl)sulfonyl-2(R)-methylpropionic acid was isolated in quantitive yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384036B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-dcef4994de94407c8aed218d4fcaf97a |
| Source note | uspto-grants-2002_05 |