Ethanolamine → HCID 2055080, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[CH2:13]([CH2:15][NH2:16])[OH:14]>>[OH:14][CH2:13][CH2:15][NH:16][S:9]([C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1)(=[O:11])=[O:10]Participants
3
Procedure
The preparation is carried out as in Example 1(a) from 413.3 g (2 mol) of p-methoxybenzenesulphonyl chloride and 128.3 g (2.1 mol) of ethanolamine. Yield: 439.3 g, i.e. 95%.
Sources & evidence
- ORD record
- ord-ecc477f7014a44448d36194a0a2c3226
- Source dataset
- uspto-grants-2002_05
- Patent number
- US06384115B1
Reaction notes
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