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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1934671Generated: October 31, 2026

3-Azidocyclopentyl benzoate → 3-Aminocyclopentyl benzoate

https://huagongshe.com/reaction/1934671

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Azidocyclopentyl benzoateHCID 22467450—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
Product3-Aminocyclopentyl benzoateHCID 2246747697%

Reaction Steps

A mixture of 3-azidocyclopentyl benzoate (411 mg) and 10% palladium on activated carbon (41.1 mg) in methanol (15 mL) was stirred under hydrogen atmosphere (4 atm) for 2 hours at ambient temperature. After removal of the catalyst, the filtrate was evaporated in vacuo to give 3-aminocyclopentyl benzoate as a pale yellow oil (354 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06384080B1
Source datasetuspto-grants-2002_05
ORD IDord-315a7e868f1841508a3d28e48f2bdbda
Source noteuspto-grants-2002_05