HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Azidocyclopentyl benzoate → 3-Aminocyclopentyl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Azidocyclopentyl benzoate | HCID 22467450 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Aminocyclopentyl benzoate | HCID 22467476 | 97% |
Reaction Steps
A mixture of 3-azidocyclopentyl benzoate (411 mg) and 10% palladium on activated carbon (41.1 mg) in methanol (15 mL) was stirred under hydrogen atmosphere (4 atm) for 2 hours at ambient temperature. After removal of the catalyst, the filtrate was evaporated in vacuo to give 3-aminocyclopentyl benzoate as a pale yellow oil (354 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384080B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-315a7e868f1841508a3d28e48f2bdbda |
| Source note | uspto-grants-2002_05 |