HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → 6-Amino-4-(3,4-dibromophenylamino)quinoline-3-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 4-[(3,4-Dibromophenyl)amino]-6-nitro-quinoline-3-carbonitrile | HCID 10114652 | — |
| Product | 6-Amino-4-(3,4-dibromophenylamino)quinoline-3-carbonitrile | HCID 10158966 | 27.3% |
Reaction Steps
Prepared from 4.90 g of 4-(3,4-dibromophenylamino)-6-nitroquinoline-3-carbonitrile and 12.4 g of SnCl2.2H2O in the same manner as EXAMPLE 378. There was obtained 1.25 g of 6-amino-4-(3,4-dibromophenylamino)quinoline-3-carbonitrile as a brown solid: mass spectrum (electrospray, m/e): M+H 416.9, 418.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384051B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-846282faa1b442b7a2b602e1e23a9305 |
| Source note | uspto-grants-2002_05 |