Trimethylsilyl iodide → HCID 10894582, compound

HRID 1935367Notes

Reaction equation

HRID 1935367 reaction equation
[CH2:1]([O:8][C:9]([N:11]1[CH2:19][CH2:18][N:17](C(OCC2C=CC=CC=2)=O)[CH2:16][CH2:15][N:14]([C:30]([O:32][CH2:33][C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)=[O:31])[CH2:13][CH2:12]1)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.I[Si](C)(C)C>>[CH2:1]([O:8][C:9]([N:11]1[CH2:19][CH2:18][NH:17][CH2:16][CH2:15][N:14]([C:30]([O:32][CH2:33][C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)=[O:31])[CH2:13][CH2:12]1)=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 85247Trimethylsilyl iodideHCID 54056276HCID 54056276, compound

Product 1

HCID 10894582HCID 10894582, compound

Procedure

From N,N′,N″-tris(benzyloxycarbonyl)-1,4,7-triazacyclononane (1.3.13.8) and iodotrimethylsilane.

Sources & evidence

ORD record
ord-faa4ca26225846acace822f65e82874c
Source dataset
uspto-grants-2002_05
Patent number
US06387891B2

Reaction notes

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