1,1-Dibromoethane → HCID 68858021, compound

HRID 1935375Notes

Reaction equation

HRID 1935375 reaction equation
[C:1]1([CH3:39])[CH:6]=[CH:5][C:4]([S:7]([N:10]2[CH2:18][CH2:17][N:16](S(C3C=CC(C)=CC=3)(=O)=O)[CH2:15][CH2:14][N:13](S(C3C=CC(C)=CC=3)(=O)=O)[CH2:12][CH2:11]2)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[Br:40]C(Br)C.[BrH:44].C(O)(=O)C>>[BrH:40].[BrH:44].[C:1]1([CH3:39])[CH:2]=[CH:3][C:4]([S:7]([N:10]2[CH2:11][CH2:12][NH:13][CH2:14][CH2:15][NH:16][CH2:17][CH2:18]2)(=[O:8])=[O:9])=[CH:5][CH:6]=1

Participants

4

Reactant 3

HCID 112011,1-DibromoethaneHCID 5641571H-1,4,7-Triazonine, octahydro-1,4,7-tris((4-methylphenyl)sulfonyl)-HCID 21893785Acetic Acid Mixture with Hydrobromic Acid

Product 1

HCID 68858021HCID 68858021, compound

Procedure

From N,N′,N″-Tris(p-toluenesulfonyl)-1,4,7-triazacyclononane (1.3.13.31) prepared from 1.3.13.18, dibromoethane and base) and HBr/acetic acid.

Sources & evidence

ORD record
ord-585c34959ba24b1cb07e79a59e17f518
Source dataset
uspto-grants-2002_05
Patent number
US06387891B2

Reaction notes

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