1H-1,4,7-Triazonine, octahydro-1,4,7-tris((4-methylphenyl)sulfonyl)- → HCID 68859289, compound

HRID 1935376Notes

Reaction equation

HRID 1935376 reaction equation
[C:1]1([CH3:39])[CH:6]=[CH:5][C:4]([S:7]([N:10]2[CH2:18][CH2:17][N:16](S(C3C=CC(C)=CC=3)(=O)=O)[CH2:15][CH2:14][N:13]([S:29]([C:32]3[CH:37]=[CH:36][C:35]([CH3:38])=[CH:34][CH:33]=3)(=[O:31])=[O:30])[CH2:12][CH2:11]2)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[BrH:40].C(O)(=O)C>>[BrH:40].[C:1]1([CH3:39])[CH:6]=[CH:5][C:4]([S:7]([N:10]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14][N:13]([S:29]([C:32]3[CH:37]=[CH:36][C:35]([CH3:38])=[CH:34][CH:33]=3)(=[O:30])=[O:31])[CH2:12][CH2:11]2)(=[O:9])=[O:8])=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 5641571H-1,4,7-Triazonine, octahydro-1,4,7-tris((4-methylphenyl)sulfonyl)-HCID 21893785Acetic Acid Mixture with Hydrobromic Acid

Product 1

HCID 68859289HCID 68859289, compound

Procedure

From N,N′,N″-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane (1.3.13.31 and HBr/acetic acid as the hydrobromide salt.

Sources & evidence

ORD record
ord-d0204fba1f49435a8a16ed2418a1112d
Source dataset
uspto-grants-2002_05
Patent number
US06387891B2

Reaction notes

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