HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Carbamic acid, (aminothioxomethyl)-, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Carbamic acid, (aminothioxomethyl)-, ethyl ester | HCID 6451585 | — |
Reaction Steps
To 0.1 mole of ethoxycarbonyl isothiocyanate in ethanol (50 ml) is added 50 ml of a 2M ethanolic solution of ammonia. After 2 hours at room temperature, the precipitated product is collected by filtration and used in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06387914B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-0c95749261bc48509cdd08da3fb70b7a |
| Source note | uspto-grants-2002_05 |