HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-N-1H-indazol-6-ylbenzenesulfonamide → HCID 178516998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-N-1H-indazol-6-ylbenzenesulfonamide | HCID 83696 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178516998 | HCID 178516998 | 16% |
Reaction Steps
The title compound was prepared in 16% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 4-amino-N-(1H-indazol-6-yl)-benzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ 12.9 (s, 1H), 11.1 (d, 1H), 10.9 (s, 1H), 10.4 (s, 1H), 9.3 (s, 1H), 8.1(d, 1H), 8.0 (s, 1H), 7.8 (d, 1H), 7.8 (d, 2H), 7.7 (d, 1H), 7.6 (d, 2H), 7.3 (s, 1H), 7.1 (d, 1H), 6.9 (d, 1H); APCI−MS m/z 487 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06387919B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-00794714074046f592430c8f74eb17b1 |
| Source note | uspto-grants-2002_05 |