HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13286111, compound → HCID 178458104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13286111 | HCID 13286111 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178458104 | HCID 178458104 | 26% |
Reaction Steps
The title compound was prepared in 26% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and N-allyl-4-aminophenylmethane sulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ 11.1 (d, 1H), 10.9 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.8 (d, 1H), 7.5 (q, 4H), 7.3 (t, 1H), 7.1 (d, 1H), 5.8 (m, 1H), 5.2 (d, 1H), 5.1 (d, 1H), 4.4 (s, 2H), 3.6 (t, 2H); APCI−MS m/z 427 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06387919B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-cf12660c032b454fa5770211673d52e3 |
| Source note | uspto-grants-2002_05 |