HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid → 3-(4-Methoxyphenyl)-2-phenylpropionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid | HCID 236698 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-(4-Methoxyphenyl)-2-phenylpropionic acid | HCID 97739 | — |
Reaction Steps
Palladium on activated carbon (10% wt., 2.77 g) was added to a solution of 3-(4-methoxyphenyl)-2-phenylacrylic acid (27.7 g, 0.11 mol) in acetic acid (1000 ml). The mixture was hydrogenated at ambient temperature. The mixture was filtered through Celite, and the solvent was evaporated. The product was recrystallized from a small amount of ethyl acetate. Melting point 220-221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388090B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-1882dce487974d0793678a129d3179de |
| Source note | uspto-grants-2002_05 |