HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 9943134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 9856251 | HCID 9856251 | — |
| Product | HCID 9943134 | HCID 9943134 | — |
Reaction Steps
reacting 3-hydroxy-5-(tert-butyldimethyl silyloxy)-(3R,5S)-cyclohexan-1-one having formula 7 with m-chloroperbezoic acid at room temperature for the period ranging from 16-24 hours, extracting with organic layer, washing with sodium metabisulphite, brine, drying and on evaporation to obtain 6-hydroxymethyl-4-(tert-butyldimethylsilyloxy)-(4S,6R)-tetrahydro-2H-2-pyranone having formula 1,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388097B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-8133deabe7f14ae5b6b89add43d3cb4a |
| Source note | uspto-grants-2002_05 |