HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Ethyl (3-(triethoxysilyl)propyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Urea | HCID 1176 | — |
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Product | Ethyl (3-(triethoxysilyl)propyl)carbamate | HCID 87367 | — |
Reaction Steps
In a 10 L distillation autoclave, 3-aminopropyltriethoxysilane (3321 g, 15 mol) are brought to reaction with urea (928 g, 15.45 mol) and ethanol (3458 g, 75 mol) at 230° C. and pressure between 35 and 23 bar. The resultant ammonia is continuously stripped out by the ethanol vapors.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388117B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-30ef601cd2bd4b389e61db91149f60fc |
| Source note | uspto-grants-2002_05 |