HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1936739Generated: October 28, 2026
2-Hydrazino-delta-2-imidazoline hydrobromide → HCID 88183062, compound
https://huagongshe.com/reaction/1936739
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Hydrazino-delta-2-imidazoline hydrobromide | HCID 3085099 | — |
| Reactant | HCID 86758080 | HCID 86758080 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 88183062 | HCID 88183062 | 109.9% |
Reaction Steps
The mixture constituted by 430 mg of the ketone prepared in Stage A, 549 mg of 4,5-dihydro-1H-imidazol-2-yl-hydrazine hydrobromide in 20 ml of butanol is heated at the temperature of 110° C. for 2 hours then evaporated under reduced pressure until 1.1 g of crude product is obtained which is purified by chromatography (Kieselgel 60, 40-63 μm) eluting with a dichloromethane/methanol mixture 90/10. 500 mg of expected product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06391904B1 |
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| Source dataset | uspto-grants-2002_05 |
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| ORD ID | ord-c3cb8f736dee4a9d85dfaab43c6507fb |
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| Source note | uspto-grants-2002_05 |
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