HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazino-delta-2-imidazoline hydrobromide → HCID 86758082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazino-delta-2-imidazoline hydrobromide | HCID 3085099 | — |
| Reactant | HCID 12235673 | HCID 12235673 | — |
| Reactant | HCID 15857342 | HCID 15857342 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86758082 | HCID 86758082 | 10.9% |
Reaction Steps
The operation is carried out as in Example 1 Stages A, B and C but using 390 mg of 4-(3-hydroxyphenyl)-2-butanone and 818 g of ethyl 4-bromo-2-[[(phenylmethoxy)carbonyl]amino]butanoate (Stage A) then, during Stage B, 380 mg of 4,5-dihydro-1H-imidazol-2-yl-hydrazine hydrobromide. The saponification stage is carried out in the presence of soda in methanol. 110 mg of expected product is obtained in the form of an E/Z mixture 45/55.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391904B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-f4919368667b4f28b6d072c4231dd551 |
| Source note | uspto-grants-2002_05 |