4-Benzyloxyaniline → HCID 22609713, compound

HRID 1936797Notes

Reaction equation

[CH2:1]([O:8][C:9]1[CH:15]=[CH:14][C:12]([NH2:13])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:16][C:17]1[C:26]2[C:21](=[CH:22][CH:23]=[C:24]([C:27]3[O:28][C:29]([CH3:32])=[N:30][N:31]=3)[CH:25]=2)[N:20]=[CH:19][N:18]=1>>[ClH:16].[CH2:1]([O:8][C:9]1[CH:10]=[CH:11][C:12]([NH:13][C:17]2[C:26]3[C:21](=[CH:22][CH:23]=[C:24]([C:27]4[O:28][C:29]([CH3:32])=[N:30][N:31]=4)[CH:25]=3)[N:20]=[CH:19][N:18]=2)=[CH:14][CH:15]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 228604-Benzyloxyaniline

HCID 226097254-Chloro-6-(5-methyl-1,3,4-oxadiazol-2-yl)quinazoline

Product 1

HCID 22609713HCID 22609713, compound

Procedure

The title compound was prepared according to Procedure A from 4-benzyloxyaniline and 4-chloro-6-(5-methyl-1,3,4-oxadiazol-2-yl)-quinazoline; δH [2H6]DMSO 11.73(1H,bs), 9.41(1H,s), 8.90(1H,s), 8.58(1H,d), 8.10(1H,d), 7.65(2H,d), 7.40(5H,m), 7.15(2H,d), 5.19(2H,s), 2.65(3H,s); m/z (M+1+) 410.

Sources & evidence

ORD record: ord-377392db111a4a09bb07f2d9b58b35e3
Source dataset: uspto-grants-2002_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06391874B1

Reaction notes

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