Methyl 2-hydroxy-3-phenylpropanoate → HCID 9850252, compound

HRID 1936893Notes

Reaction equation

HRID 1936893 reaction equation
[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][C:26]([OH:29])=[CH:25][CH:24]=2)=[CH:19][CH:18]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C[O:31][C:32](=[O:42])[CH:33]([CH2:35][C:36]1[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=1)O>>[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:24]=[CH:25][C:26]([O:29][CH:33]([CH2:35][C:36]3[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=3)[C:32]([OH:42])=[O:31])=[CH:27][CH:28]=2)=[CH:19][CH:18]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 518800Methyl 2-hydroxy-3-phenylpropanoateHCID 10548559HCID 10548559, compound

Product 1

HCID 9850252HCID 9850252, compound

Procedure

The title compound was prepared from 4′-(2-benzyl-benzo[b]-thiophen-3-yl)-biphenyl-4-ol, and 3-phenyllactic acid methyl ester, in substantially the same manner, as described in Example 1, steps g-h, and was obtained as a white solid, mp 165-167° C.; MS m/e 540 (M+);

Workup

  1. customwas obtained as a white solid, mp 165-167° C.

Sources & evidence

ORD record
ord-d86a355d4f504fb882c440377cff3988
Source dataset
uspto-grants-2002_05
Patent number
US06391897B2

Reaction notes

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