Acetone → Dipentaerythritol

HRID 1936962Notes

Reaction equation

HRID 1936962 reaction equation
CC(CC(CNC(OCCOC(C(C)=C)=O)=O)(C)C)CCN[C:6](OCCOC(C(C)=C)=O)=[O:7].C([O:39][CH:40]([C:42]1[C:43]([O:67][C:68](=O)C(C)=C)(C([O-])=O)C(C=C[C:50]=1[O:51]C1C=C(C([O-])=O)C(=CC=1)C([O-])=O)C([O-])=O)C)(=O)C(C)=C.C12(C)C(C)(C)C(CC1)C(=O)[C:74]2=[O:75].[CH2:85]([OH:87])[CH3:86].C[C:89](C)=[O:90]>>[OH:87][CH2:85][C:86]([CH2:89][OH:90])([CH2:68][O:67][CH2:43][C:42]([CH2:40][OH:39])([CH2:50][OH:51])[CH2:74][OH:75])[CH2:6][OH:7]

Participants

6

Reactant 5

HCID 180AcetoneHCID 702EthanolHCID 25208Bornane-2,3-dioneHCID 170472Urethane dimethacrylateHCID 867580841,2'-Bis-methacryloyloxy-ethyl-4,4'-oxydiphthalate

Product 1

HCID 31352Dipentaerythritol

Procedure

8.78 grams 2,7,7,9,15-pentamethyl-4, 13-dioxo-3, 14-dioxa 5,12-diaza-hexadecane-1, 16diyldimetylate (UDMA); 3.33 grams 7, 7, 9 63, 63, 65-hexamethyl-4, 13, 60, 69-tetra-xo-3, 14, 19, 24, 29, 34, 39, 44, 49, 54, 59, 70-dodecanoxa-5, 12, 61, 68-tetra-aza-doheptacontane-1, 72-diyl-dimethacrylate resin; 5.04 grams a mixture of 1,1′, 2,2′ and 1,2′-bis-methacryloyloxy-ethyl-4,4′-oxydiphthalate (OEMA); 0.20 grams camphorquinone (CQ); 0.60 grams ethyl-4,N,N-dimethylaminobenzoate (EDAB); 0.10 grams butylated hydroxytoluene (BHT); 14.83 grams ethanol and 59.14 grams acetone are mixed at 23° C. for 30 minutes to form a Self-Priming Metal Adhesive.

Sources & evidence

ORD record
ord-00b7d83f686840b79c3766064016df64
Source dataset
uspto-grants-2002_05
Patent number
US06391940B1

Reaction notes

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