참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phosgene | HCID 6371 | — |
| 반응물 | Cyclohexane, (ethenyloxy)- | HCID 75129 | — |
| 생성물 | 3-Cyclohexyloxyacryloyl chloride | HCID 53968361 | 88% |
반응 단계
50 g (0.5 mol) of phosgene are condensed into a stirred apparatus fitted with −78° C.-cooling. Over a period of 3 hours, 50.5 g (0.4 mol) of cyclohexyl vinyl ether are subsequently added dropwise at 20° C. The mixture is then stirred at 50° C. for 5 hours. The excess phosgene is flushed out with nitrogen, and the crude product is worked up by distillation. At 110° C./2.5 mbar, 66.4 g (88%) of the product of value were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06392058B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_05 |
|---|
| ORD ID | ord-dffae57b497f45268a46a5de7032e4f8 |
|---|
| 출처 메모 | uspto-grants-2002_05 |
|---|
