HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentaneethanol → HCID 22462756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentaneethanol | HCID 69833 | — |
| Reactant | HCID 22462795 | HCID 22462795 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22462756 | HCID 22462756 | 58% |
Reaction Steps
By essentially following the conditions described in Example 2, Part A, the title compound was prepared from 6-benzyloxy-3-[3-methyl-4-[(1-pyrrolidinyl)methyl]benzyl]-2-(4-hydroxyphenyl)benzo[b]thiophene (Example 8; Part C) and 2-cyclopentylethanol in 58% yield following radial chromatography (SiO2; 5% THF and 2.5% TEA in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391901B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-55600375171e4b9fb40686b4aa34677f |
| Source note | uspto-grants-2002_05 |