Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Adamantane | HCID 9238 | — |
| Catalyst | Cobalt(2+) | HCID 104729 | — |
| Product | 1-Adamantyl acetate | HCID 519973 | — |
| Product | HCID 11807143 | HCID 11807143 | — |
Reaction Steps
A mixture of 10 mmole of adamantane, 1 mmole of NHPI, 0.05 mmole of cobalt(II) acetylacetonato (Co(AA)2) and 25 mL of acetic acid was stirred for 6 hours at 75° C. under an oxygen atmosphere to give 1-acetyloxyadamantane and 1,3-diacetyloxyadamantane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06392104B1 |
|---|
| Source dataset | uspto-grants-2002_05 |
|---|
| ORD ID | ord-98bc4acfa659409dbe71969f7f23d17b |
|---|
| Source note | uspto-grants-2002_05 |
|---|
