HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → Tricyclo(3.3.1.13,7)decane-1-carboxylic acid, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Tricyclo(3.3.1.13,7)decane-1-carboxylic acid, methyl ester | HCID 136553 | — |
Reaction Steps
In the presence of an acid catalyst (p-toluenesulfonic acid), 1-carboxyadamantane obtained in Example 2 was allowed to react with an excess amount of methanol to give 1-methoxycarbonyladamantane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06392104B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-19ce1783c9d1447f9f19120b592b80f8 |
| Source note | uspto-grants-2002_05 |