HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 22463609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | HCID 12070473 | HCID 12070473 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22463609 | HCID 22463609 | 85% |
Reaction Steps
In toluene (100 mL) was dissolved 10 mmole of 1-acetyloxy-3-aminoadamantane obtained by the method of Example 15. To the resultant solution was added 12 mmole of phosgene at room temperature and the mixture was stirred for 6 hours. As a result, the conversion of 1-acetyloxy-3-aminoadamantane was 95% and 1-acetyloxy-3-isocyanatoadamantane (yield 85%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06392104B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-717c02905c3b410cbb43031bbd164d4c |
| Source note | uspto-grants-2002_05 |