HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 178447137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21337830 | HCID 21337830 | — |
| Product | HCID 178447137 | HCID 178447137 | — |
Reaction Steps
In an analogous fashion to Example 1b the product was prepared using 6.13 g (20 mmols) of 2-hydroxy-5-(4-oxocyclohexyl)benzoic acid pentyl ester and 0.76 g (200 mmols) NaBH4. Recrystallisation from isopropanol gave the 2-hydroxy-5-(trans-4-hydroxycyclohexyl)benzoic acid pentyl ester product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395351B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-a12f397c02154a8692206240da2852f3 |
| Source note | uspto-grants-2002_05 |