HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-D-Ala-Gly-NH2 → (S)-Benzyl (1-((2-amino-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-D-Ala-Gly-NH2 | HCID 11437420 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (S)-Benzyl (1-((2-amino-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate | HCID 10937159 | — |
Reaction Steps
Z-D-Ala-Gly-NH2 (21) (Richman et al., Int. Peptide Protein Res., 25:648-662 (1985), which is hereby incorporated by reference): 1H and 13C NMR data are identical to (8). HRMS (FAB+) MH+ calcd 280.1297 found 280.1298; [α]27D+10.5 (c 0.72, MeOH); lit. [α]D=+10.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395532B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-947537ce567e4d0dafb707f21d5e3345 |
| Source note | uspto-grants-2002_05 |