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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1937306Generated: October 31, 2026

5,6-Dimethylbenzimidazole → HCID 18417276, compound

https://huagongshe.com/reaction/1937306

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5,6-DimethylbenzimidazoleHCID 675—
ReactantDistearylmethylamineHCID 77709—
ReactantTris(pentafluorophenyl)boraneHCID 582056—
SolventTolueneHCID 1140—
ProductHCID 18417276HCID 18417276—

Reaction Steps

5,6-dimethylbenzimidazole (0.2855 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for 16 hours. The volatiles were then stripped under vacuum. Yield, 3.060 g, 91.84 percent.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06395671B2
Source datasetuspto-grants-2002_05
ORD IDord-58c6a491e03d4031aab15805c106fb51
Source noteuspto-grants-2002_05