HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Dimethylbenzimidazole → HCID 18417276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Dimethylbenzimidazole | HCID 675 | — |
| Reactant | Distearylmethylamine | HCID 77709 | — |
| Reactant | Tris(pentafluorophenyl)borane | HCID 582056 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18417276 | HCID 18417276 | — |
Reaction Steps
5,6-dimethylbenzimidazole (0.2855 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for 16 hours. The volatiles were then stripped under vacuum. Yield, 3.060 g, 91.84 percent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395671B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-58c6a491e03d4031aab15805c106fb51 |
| Source note | uspto-grants-2002_05 |