HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 12016976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 7H-Pyrrolo(2,3-d)pyrimidine, 4-chloro- | HCID 5356682 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 12016976 | HCID 12016976 | 16% |
Reaction Steps
Utilizing a procedure analogous to that described in Example 1, this product was prepared in 16% yield from 4-Chloro-7H-pyrrolo[2,3-d]pyrimidine (1.0 eq) and aniline (5.0 eq) in pyridine. (M.P. 234-236° C.; GC-MS: 211(MH+); anal. RP18-HPLC RT: 3.11 min.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395733B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-cd437d869cd44d8c8d67ddc606f669f6 |
| Source note | uspto-grants-2002_05 |