HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21925692, compound → HCID 21925676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21925692 | HCID 21925692 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 21925676 | HCID 21925676 | 73.4% |
Reaction Steps
Dimethyl 2-[2-nitro-4-(3-trifluoroacetamidophenyl)phenyl]malonate (4.4 g) was refluxed overnight in 50 mL 6 N hydrochloric acid. The reaction mixture was cooled to room temperature and the solids were collected by vacuum filtration, washed with water, and dried under vacuum to give 2.7 g (73% yield) of 2-[2-nitro-4-(3-trifluoroacetamidophenyl)phenyl] acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395734B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-931c93c1b2cd4cc6acf32b082a45f7fa |
| Source note | uspto-grants-2002_05 |