2-(Tributylstannyl)-1,3-thiazole → HCID 22461270, compound

Participants

Reaction Steps

In the same way as described in Example 15, Step 4 using 3-bromo-1-(6-chloropyridin-2-yl)-6,6-dimethyl-1,2,3,4-tetrahydroindol-4-one and 2-tributylstannylthiazole, the title compound (35 mg; 13%) was isolated as a yellow solid. 1H NMR (400 MHz, CDCl3) δ 1.21 (6H,s), 2.55 (2H,s), 3.24 (2H,s) 7.35 (1H,d, J=3.1 Hz), 7.50-7.53 (2H,m), 7.81 (1H,d, J=3.1 Hz), 7.97-8.02 (3H,m), 8.20 (1H,d, J=7.8 Hz). MS (ES+) 407 (M+1).

Provenance & Evidence