Bromomethyl 4-methoxyphenyl ketone → HCID 12695073, compound

HRID 1937641Notes

Reaction equation

HRID 1937641 reaction equation
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:9][C:10]([C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=1)=[O:11]>>[C:1]1([S:7][CH2:9][C:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)=[O:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 4965Bromomethyl 4-methoxyphenyl ketoneHCID 7969Thiophenol

Product 1

HCID 12695073HCID 12695073, compound

Procedure

Thiophenol and 2-bromo-4′-methoxyacetophenone were converted to the title compound by the procedure of Preparation 1. mp 83° C.-85° C. EA calculated for C15H14O2S: C, 69.74; H, 5.46. Found: C, 69.52; H, 5.48.

Sources & evidence

ORD record
ord-f2901440d1cd4068b5512139c4659353
Source dataset
uspto-grants-2002_05
Patent number
US06395769B1

Reaction notes

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