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HRID 1937648作成日:2026年10月25日

Acrylamide → n-Decylacrylamide Acrylamid

https://huagongshe.com/reaction/1937648

反応式

関与物質

役割名称HCID仕込み量
反応物AcrylamideHCID 6579—
反応物2-MethylidenedodecanamideHCID 21275879—
溶媒IsopropanolHCID 3776—
生成物n-Decylacrylamide AcrylamidHCID 21275878—

反応条件

温度75 °C

反応手順

To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammoniumethylacrylate chloride, 8.06 g of n-decylacrylamide, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ˜15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06395777B2
出典データセットuspto-grants-2002_05
ORD IDord-75de3cdfc8b14e4385c206ef40134096
出典メモuspto-grants-2002_05