Chloropentafluorobenzene → HCID 178505971, compound
Reaction equation
[F:1][C:2]1[C:7](Cl)=[C:6]([F:9])[C:5]([F:10])=[C:4]([F:11])[C:3]=1[F:12].C([Mg:16][Br:17])(C)C>>[F:1][C:2]1[C:7]([Mg:16][Br:17])=[C:6]([F:9])[C:5]([F:10])=[C:4]([F:11])[C:3]=1[F:12]Participants
3
Procedure
The process according to claim 8 wherein the step (a) pentafluorochlorobenzene is reacted with isopropylmagnesium bromide in a mole ratio range from about 1:1 to 2:1 in a dialkyl ether solvent to provide pentafluorophenylmagnesium bromide.
Sources & evidence
- ORD record
- ord-f35157be4385460fbea0e08928447228
- Source dataset
- uspto-grants-1997_12
- Patent number
- US05693261
Reaction notes
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