HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitro-7-(5-ethyl-2-pyridylmethoxy)quinoline → 3-Amino-7-(5-ethyl-2-pyridylmethoxy)quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitro-7-(5-ethyl-2-pyridylmethoxy)quinoline | HCID 21469290 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Amino-7-(5-ethyl-2-pyridylmethoxy)quinoline | HCID 21469277 | — |
Reaction Steps
In ethanol (20 mL) was suspended 3-nitro-7-(5-ethyl-2-pyridylmethoxy)quinoline (700 mg, 2.26 mmol.), and to the suspension was added platinum oxide (80 mg). Then, catalytic reduction was performed for 3 hours. After the completion of reaction was confirmed, the reaction mixture was filtered over Celite®, and the filtrate was placed under reduced pressure to give the desired compound as residual oil in a quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693651 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-6cdf47ffa16846fcb5a9aa3de90c89dd |
| Source note | uspto-grants-1997_12 |