HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 86751680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 86751679 | HCID 86751679 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86751680 | HCID 86751680 | — |
Reaction Steps
Combine (E and Z)-1-(4-chlorobutoxy)phenyl-1,2-diphenyl ethylene (20.2 mol) and chloroform (60 L). Add N-chlorosuccinimide (7 kg, 52.4 mol). Heat to reflux. After 18 hours, cool to ambient temperature and add water. Separate the organic layer and extract with aqueous saturated sodium carbonate solution. Separate the organic layer and evaporate in vacuo to give (E and Z)-1-(4-chlorobutoxy)phenyl-2-chloro-1,2-diphenyl ethylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693674 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-31e00a19c93042ef9f184915ed57fccd |
| Source note | uspto-grants-1997_12 |