HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 4262649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 4-Nitrophthalic acid anhydride | HCID 230976 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 4262649 | HCID 4262649 | 89% |
Reaction Steps
A mixture of 4-nitrophthalic anhydride (18 g, 93.3 mmol) and phenethylamine (11.5 g, 95 mmol) in toluene (250 mL) was heated to reflux. After 2.5 h, the mixture was concentrated to solid residue, which was triturated and filtered to yield the title compound (24.5 g, 89%). Mp 142°-3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693636 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-26fb1fc58ffb4dc7bb9f9a044ef0724d |
| Source note | uspto-grants-1997_12 |