Aniline → HCID 54078375, compound

HRID 1938784Notes

Reaction equation

HRID 1938784 reaction equation
[N:1]([C:4](=[CH:10][N:11]([CH3:13])[CH3:12])[C:5]([O:7][CH2:8][CH3:9])=[O:6])=[C:2]=[O:3].[NH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>C1(C)C=CC=CC=1>[C:5]([C:4]([NH:1][C:2]([NH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:3])=[CH:10][N:11]([CH3:12])[CH3:13])([O:7][CH2:8][CH3:9])=[O:6]

Participants

4

Reactant 2

HCID 6115AnilineHCID 54395864HCID 54395864, compound

Product 1

HCID 54078375HCID 54078375, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of Ethyl 2-isocyanato-3-(dimethylamino)-propenoate (5.52 g) in toluene (250 mL) was added aniline (2.79 g). The reaction was stirred at room temperature for 30 min. The resulting solid was collected and dried to yield N-(1-Carboethoxy-2-dimethylaminovinyl)-N'-phenyl urea as a white solid.

Workup

  1. customThe resulting solid was collected
  2. customdried

Sources & evidence

ORD record
ord-547ee25389014f3487e003acb21ab635
Source dataset
uspto-grants-1997_12
Patent number
US05693801

Reaction notes

Loading…