HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N,N'-dibenzylethylenediaminium N,N'-diacetyl-L-cystinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzathine | HCID 8793 | — |
| Reactant | N,N'-Diacetyl-L-cystine | HCID 6995101 | — |
| Product | N,N'-dibenzylethylenediaminium N,N'-diacetyl-L-cystinate | HCID 131718839 | — |
Reaction Steps
To a 63% solution of N,N'-diacetyl-L-cystine in water (67 mmole, 21.8 g) was added N,N'-dibenzylethylenediamine (67 mmole, 16.0 g). The exothermic reaction gave a slightly oily product which could be recrystallised from water to give 12.0 g (32%) of the title substance as white crystalline needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693858 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-c665ec9b4f5246d989b83791ec24f688 |
| Source note | uspto-grants-1997_12 |