HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 18630101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | HCID 18630361 | HCID 18630361 | — |
| Solvent | Carbon Dioxide | HCID 280 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18630101 | HCID 18630101 | — |
Reaction Steps
2-Chloro-6-trimethylsilylbenzoyl isocyanate (1.3 g, 5 mmol) was dissolved in 40 mL toluene and isopropyl amine (1 g) added over a period of 30 seconds. After stirring 30 min, the solvent was removed to yield an oil. The oil was dissolved in hexane and cooled in dry ice to yield 1.2 g of crystals of the title compound. m.p. 113°-116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693667 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-dd673948c8604249ab98928c65aacf19 |
| Source note | uspto-grants-1997_12 |