HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium → Potassium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | Yttrium trichloride | HCID 10198055 | — |
| Reactant | Potassium ethoxide | HCID 23670592 | — |
| Reactant | HCID 178473702 | HCID 178473702 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Potassium Chloride | HCID 4873 | — |
| Product | HCID 14178979 | HCID 14178979 | — |
Reaction Steps
Dissolve anhydrous salts such as Yttrium chloride (YCl3) in pure ethanol. Add a known quantity of potassium to ethanol and make potassium ethoxide, KOC2H5. Mix this with YCl3 in ethanol and stir. Under refluxing, a clear solution of yttrium ethoxide and a precipitate of potassium chloride is obtained. The dopant Eu can similarly be added to the Yttrium chloride in ethanol at first and this reaction would form Yttrium europium ethoxides. The ethoxides can then be hydrolyzed by adding a solution of ammonia at room temperature. These products are separated and can then be deposited by various means outlined earlier.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05695809 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-dde17c81405249159a0fe2344e0d6407 |
| Source note | uspto-grants-1997_12 |