3,5-Dichlorophenyl isocyanate → HCID 54332053, compound

HRID 1939281Notes

Reaction equation

HRID 1939281 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]=[C:10]=[O:11])[CH:5]=[C:6]([Cl:8])[CH:7]=1.[CH3:12][O:13][C:14]1[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:15]=1[NH2:16]>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([NH:9][C:10]([NH:16][C:15]2[CH:17]=[C:18]([C:21]([F:23])([F:24])[F:22])[CH:19]=[CH:20][C:14]=2[O:13][CH3:12])=[O:11])[CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

4

Reactant 2

HCID 944603,5-Dichlorophenyl isocyanateHCID 6006372-Methoxy-5-(trifluoromethyl)aniline

Product 1

HCID 54332053HCID 54332053, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent2×

Procedure

3,5-dichlorophenyl isocyanate (0.94 g, 5.0 mmol) in toluene (10 ml) was added to a solution of 2-methoxy-5-(trifluoromethyl)aniline (0.96 g, 5.0 mmol) in toluene (10 ml). The reaction was stirred at RT for 1 hour and the product filtered off. 1.20 (63%) of the title compound was isolated.

Workup

  1. filtrationthe product filtered off

Sources & evidence

ORD record
ord-a764871c37234e4dac9571bbb725d5f7
Source dataset
uspto-grants-1997_12
Patent number
US05696138

Reaction notes

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