HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride → HCID 53710724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride | HCID 23393 | — |
| Reactant | 2-[2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]ethyl]-2H-1,4-benzoxazin-3(4H)-one | HCID 12048020 | — |
| Product | HCID 53710724 | HCID 53710724 | — |
Reaction Steps
2-(2-tert-Butyldimethylsiloxyethyl)-3,4-dihydro-3-oxo-2H-1,4-benzoxazine was alkylated with 2-chloromethylpyridine by method F and the crude product was deprotected by method H without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05696117 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-d7362c82d4474ee1a876df8ba3b927bd |
| Source note | uspto-grants-1997_12 |