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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1939372Generated: November 1, 2026

alpha-Chloro-m-nitrotoluene → HCID 54348374, compound

https://huagongshe.com/reaction/1939372

Reaction equation

Participants

RoleNameHCIDCharge
Reactantalpha-Chloro-m-nitrotolueneHCID 12078—
Reactant2-[2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]ethyl]-2H-1,4-benzoxazin-3(4H)-oneHCID 12048020—
ProductHCID 54348374HCID 54348374—

Reaction Steps

The intermediate silyl protected alcohol was prepared from 2-(2-tert-butyldimethylsiloxyethyl)-3,4-dihydro-3-oxo-2H-1,4-benzoxazine by Method F, alkylating with 3-nitrobenzyl chloride. Deprotection to the indicated product was carried out by method I.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05696117
Source datasetuspto-grants-1997_12
ORD IDord-2b3e76848f7d49b4af6da25a7e9b17ef
Source noteuspto-grants-1997_12