HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 4-(2,2-Dimethyl-1,3-dioxolan-4-yl)butan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 1,2,6-Hexanetriol | HCID 7823 | — |
| Product | 4-(2,2-Dimethyl-1,3-dioxolan-4-yl)butan-1-ol | HCID 236682 | — |
Reaction Steps
15 g (112 mmol) of 1,2,6-hexanetriol were dissolved together with 0.5 g of FeCl3 in 1 l of acetone and boiled under reflux for 7 h. The mixture was filtered, and excess acetone was removed by distillation, resulting in the product in pure form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05696248 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-dcba100521dc440f82d5098f356e0e1a |
| Source note | uspto-grants-1997_12 |