HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1939877Generated: October 25, 2026
2-Heptanol → (1-Methyl)hexyl 2-pyridyloxyacetate
https://huagongshe.com/reaction/1939877
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Heptanol | HCID 10976 | — |
| Reactant | Ethyl 2-(pyridin-2-yloxy)acetate | HCID 21464941 | — |
| Catalyst | Titanium isopropoxide | HCID 11026 | — |
| Product | (1-Methyl)hexyl 2-pyridyloxyacetate | HCID 21464939 | 90% |
Reaction Steps
5.0 g (28 mmol) of ethyl 2-pyridyloxyacetate were suspended in 100 ml of 2-heptanol, 1 ml of titanium tetraisopropoxide were added, and the mixture was stirred for 4 hours at 120° C. The excess 2-heptanol was subsequently distilled off under an oil pump vacuum, and the residue was purified by column chromatography. 6.2 g (90% of theory) of (1-methyl)hexyl 2-pyridyloxyacetate were obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05698539 |
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| Source dataset | uspto-grants-1997_12 |
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| ORD ID | ord-240782b943054781b8e440bec68b2785 |
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| Source note | uspto-grants-1997_12 |
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