2-Chloropyridine → HCID 15177822, compound

HRID 1939880Notes

Reaction equation

HRID 1939880 reaction equation
Cl[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[N:8]1[CH:13]=[CH:12][CH:11]=[C:10]([CH2:14][CH:15]2[CH:24]([OH:25])[C:23]3[C:18](=[CH:19][CH:20]=[C:21]([OH:26])[CH:22]=3)[O:17][CH2:16]2)[CH:9]=1>>[N:8]1[CH:13]=[CH:12][CH:11]=[C:10]([CH2:14][C@H:15]2[C@@H:24]([OH:25])[C:23]3[C:18](=[CH:19][CH:20]=[C:21]([O:26][C:2]4[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=4)[CH:22]=3)[O:17][CH2:16]2)[CH:9]=1

Participants

3

Reactant 2

HCID 79772-ChloropyridineHCID 15181191HCID 15181191, compound

Product 1

HCID 15177822HCID 15177822, compound

Procedure

By the method of Example 1, 2-chloropyridine and 3-(3-pyridylmethyl)-4,6-chromandiol were converted to present title product in like yield; mp 67°-68° C.; IR(CHCl3) 1598; 1491 cm-1.

Sources & evidence

ORD record
ord-180ca93c360c410898aaf1d6e3f7dca7
Source dataset
uspto-grants-1997_12
Patent number
US05698550

Reaction notes

Loading…