HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Chlorophenyl)-cyclohex-3-enecarboxylic acid → 4-(4-Chlorophenyl)cyclohexane-1-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Chlorophenyl)-cyclohex-3-enecarboxylic acid | HCID 21465099 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(4-Chlorophenyl)cyclohexane-1-carboxylic acid | HCID 2735792 | 99.2% |
Reaction Steps
Reduce a solution of the product of STEP 2 (1.36 g) in EtOAc (50 mL) over 10% Pd/C under H2 (50 psi) for 14 h. Filter the catalyst and concentrate the solution to give the title compound (1.36 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698548 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-70d906e12c1a4e5ab67fdea5055f68ca |
| Source note | uspto-grants-1997_12 |