HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 21465086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 21465085 | HCID 21465085 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21465086 | HCID 21465086 | 94.3% |
Reaction Steps
To a solution of the product of STEP 2 (1.26 g) in MeOH (20 mL), add water (5 mL) and LiOH (0.61 g) and stir overnight at ambient temperature. Dilute the reaction mixture with water and extract with Et2O. Acidify the aqueous layer with conc.HCl and extract with EtOAc. Separate the organic layer, wash with water and brine, and concentrate to obtain the title compound (1.06 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698548 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-4afd939f4f8d46f781da626a92986ce8 |
| Source note | uspto-grants-1997_12 |