HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → 7-chloroacetyl-2,3-dihydro-4H-1,4-benzoxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 2H-1,4-benzoxazin-3(4H)-one | HCID 72757 | — |
| Reactant | 7-(2-(3-Benzylpiperidino)-1-oxoethyl)-2,3-dihydro-1,4-benzoxazin-3-one | HCID 21465137 | — |
| Product | 7-chloroacetyl-2,3-dihydro-4H-1,4-benzoxazin-3-one | HCID 21465147 | — |
Reaction Steps
from 7-(2-(3-benzylpiperidino)-1-oxoethyl)-2,3-dihydro-1,4-benzoxazin-3-one ("F"; obtainable by reaction of 2,3-dihydro-1,4-benzoxazin-3-one with chloroacetyl chloride to give 7-chloroacetyl-2,3-dihydro-4H-1,4-benzoxazin-3-one ("G"), then reaction with 3-benzylpiperidine):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698553 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-4e04ffd3ae594b2a883c14fb14232616 |
| Source note | uspto-grants-1997_12 |