HCID 11858098, compound → HCID 21465327, compound

HRID 1939960Notes

Reaction equation

HRID 1939960 reaction equation
[CH2:1]([N:3]([CH2:17][CH3:18])[CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:16]=[CH:15][C:12]([C:13]#[N:14])=[CH:11][CH:10]=1)[CH3:2].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH2:17]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][NH2:14])=[CH:11][CH:10]=1)[CH3:18]

Participants

3

Reactant 2

HCID 11858098HCID 11858098, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 21465327HCID 21465327, compound

Procedure

According to a similar manner as that in Reference Example 78, 4-[4-(diethylamino)butoxy]benzonitrile obtained above was reduced by lithium aluminium hydride to give the title compound (quantitative). This compound was used in the subsequent reaction without further purification.

Workup

  1. customobtained

Sources & evidence

ORD record
ord-b8243fa5c43d41beb62e8efd3e5ba4fd
Source dataset
uspto-grants-1997_12
Patent number
US05698560

Reaction notes

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